Temporal Aroma Delivery from Milk Systems Containing 0−5% Added Fat, Observed by Free Choice Profiling, Time Intensity, and Atmospheric Pressure Chemical Ionization−Mass Spectrometry Techniques

Abstract

A temporal aroma delivery from milk systems containing 0, 0.5, or 5% added fat and flavored with seven-component strawberry flavoring and linalool was observed by free choice profiling (FCP), time intensity (TI), and atmospheric pressure chemical ionization-mass spectrometry (APCI-MS) techniques. A suppressing effect of fat on the volatility of the relatively nonpolar compound linalool was observed by all methods, but only slight evidence (with the TI method) of the effect of fat on the overall strawberry (based on more polar compounds) intensity was found. With the TI method, the strawberry aroma of the fattiest sample lingered the longest, but no temporal differences were found in the release of linalool. The APCI-MS results showed no effect of fat on the temporal release of ethyl butyrate (mainly responsible for the strawberry note), but linalool of the sample containing 5% fat was found to be the most persistent. However, the effect on linalool was observed using a slightly different sampling technique than in the TI. Overall, FCP, TI, and APCI-MS showed parallel results for the effect of fat on the intensity of aroma, but temporal release data only partly supported the theory that fat slows down the release of aroma compounds and their perception.