Journal of Applied Physics · 2008 · 15 citations · 22 references
Natural SciencesMaterials EngineeringMaterials ScienceCrystal StructureMaterials CharacterizationMechanical Behavior Of MaterialsCrystallographyDeformation MechanismsDislocation MechanicsX-ray CrystallographyX-ray Data AnalysisX-ray DiffractionDislocation Burgers VectorsDislocation CharacterizationDislocation InteractionsDislocation PropagationDislocationsScrew DislocationsSilicon CarbideX-ray Topography
The x-ray topography by using highly coherent beam obtained at third-generation synchrotron facilities can provide higher spatial resolution and higher lattice-distortion sensitivity than those by former-generation facilities. Here, we report the direct determination of the Burgers vector senses and magnitudes of elementary dislocations in a high-quality silicon carbide single crystal using white x-ray section topography with a long sample-to-film distance. Our data strongly indicate that there are very weak but extraordinarily long-range elastic interactions between elementary screw dislocations. Those interactions govern dislocation-propagation behavior and the distribution of dislocations. Moreover, we found that white x-ray projection topography with a long sample-to-film distance can also be a powerful tool to effectively examine the detailed structure of elementary dislocations in single crystals.
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Ultrahigh-quality silicon carbide single crystals
Daisuke Nakamura, Itaru Gunjishima, S. Yamaguchi et al. · Nature · 2004 · 423 citations