Use of a soft sensor for the fast estimation of dried cake resistance during a freeze-drying cycle

HANDBOOK OF INDUSTRIAL DRYING

Carl W. Hall · Drying Technology · 1988 · 562 citations

Industrial Drying, Mechanical Engineering, Thermal Processing +1

Determination of End Point of Primary Drying in Freeze-Drying Process Control

Sajal M. Patel, Takayuki Doen, Michael J. Pikal · AAPS PharmSciTech · 2010 · 265 citations · Full text

Primary Drying, Desiccation, Food Engineering +4

Heat and mass transfer scale-up issues during freeze drying: II. Control and characterization of the degree of supercooling

Shailaja Rambhatla, Roee Ramot, Chandan Bhugra et al. · AAPS PharmSciTech · 2004 · 236 citations · Full text

Materials Science, Freeze-thaw Cycling, Heat Transfer Process +11

Use of laboratory data in freeze drying process design: heat and mass transfer coefficients and the computer simulation of freeze drying.

Pikal Mj · PubMed · 1985 · 200 citations

Engineering, Mechanical Engineering, Thermal Processing +20

Physical Chemistry of Freeze-drying: Measurement of Sublimation Rates for Frozen Aqueous Solutions by a Microbalance Technique

Michael J. Pikal, Saroj Shah, David E. Senior et al. · Journal of Pharmaceutical Sciences · 1983 · 195 citations

Freeze-thaw Cycling, Engineering, Desiccation +9