Journal of Synchrotron Radiation · 2017 · 10 citations · 24 references
Natural SciencesMaterials SciencePhysicsCondensed Matter PhysicsElectronic MaterialsSemiconductor MaterialsCrystallographyNanowiresStacking FaultsTransmission Electron MicroscopyX-ray CrystallographyX-ray DiffractionDiffraction Signatures Of Stacking FaultsElectron DensityElectron Density DistributionsMetalorganic Vapor Phase EpitaxyNanowire CharacterizationSemiconductor CrystallographySemiconductor NanowiresStacking Faults In Semiconductors
Coherent X-ray diffraction was used to measure the type, quantity and the relative distances between stacking faults along the growth direction of two individual wurtzite GaAs nanowires grown by metalorganic vapour epitaxy. The presented approach is based on the general property of the Patterson function, which is the autocorrelation of the electron density as well as the Fourier transformation of the diffracted intensity distribution of an object. Partial Patterson functions were extracted from the diffracted intensity measured along the [000\bar{1}] direction in the vicinity of the wurtzite 00\bar{1}\bar{5} Bragg peak. The maxima of the Patterson function encode both the distances between the fault planes and the type of the fault planes with the sensitivity of a single atomic bilayer. The positions of the fault planes are deduced from the positions and shapes of the maxima of the Patterson function and they are in excellent agreement with the positions found with transmission electron microscopy of the same nanowire.
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