Publication | Open Access
Resolution and absolute configuration assignment of a chiral hemicryptophane molecular cage
29
Citations
20
References
2010
Year
Medicinal ChemistrySemipreparative HplcBioorganic ChemistryAbsolute ConfigurationBiochemistryEngineeringNatural SciencesHeterocyclicAbsolute Configuration AssignmentEnantioselective SynthesisIsolated EnantiomerMolecular BiologyConformational StudySpectra-structure CorrelationOrganic ChemistryHeterocycle ChemistryMolecular RecognitionBiophysics
The racemic hemicryptophane molecular cage 2 was resolved by semipreparative HPLC on Whelk-O1 column. The absolute configuration of each isolated enantiomer was established from the analysis of their circular dichroism spectra and assigned as P-(+)-2 and M-(-)-2.
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