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A multi-technique approach using LC–NMR, LC–MS, semi-preparative HPLC, HR–NMR and HR–MS for the isolation and characterization of low-level unknown impurities in GW876008, a novel corticotropin-release factor 1 antagonist

BiochemistryLow-level Unknown ImpuritiesMedicineBioanalysisMass SpectrometryAnalytical ChemistryMulti-technique ApproachLiquid ChromatographySolution Nmr SpectroscopyPharmacologySemi-preparative HplcChromatographyDrug Analysis