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A Low-Power Pressure- and Temperature-Programmable Micro Gas Chromatography Column
69
Citations
12
References
2007
Year
Experimental ResultsChemical EngineeringEngineeringGas ChromatographyMicrofabricationSuspended ColumnMedicineAnalytical MicrosystemsMass SpectrometryTemperature ProgrammingAnalytical ChemistryLiquid ChromatographyClinical ChemistryChemistryChromatographic AnalysisMicrofluidicsChromatography
This paper presents the theory, fabrication, and experimental results for a high-performance low-power micro gas chromatography column. The suspended-dielectric 1-m-long column is split into two sections, permitting independent pressure and temperature programming. Integrated column heaters have a mean resistance of 16.8 kOmega and a temperature coefficient of resistance of 431 ppm/degC. The suspended column requires 11 mW to raise its temperature by 100degC in vacuum (1 mtorr). The column separates ten volatile organic compounds in 52 s and four chemical warfare agent simulants and an explosive simulant in 60 s.
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