Journal of Separation Science · 2012 · 21 citations · 24 references
PharmacyFood SciencePlant SciencesChromatographic AnalysisFood AnalysisSeparation ScienceAnalytical ChromatographyExtraction TechniquesMedicinal PlantsMetabolite ExtractionSolvent ExtractionSupercritical Fluid ExtractionCentral Composite DesignsEssential Oil AnalysisEssential Oil ExtractionExtraction Of Essential OilsExtraction Of Organic CompoundsExtraction Time OptimizationOil ExtractionPharmaceutical Extraction
Essential oil components were extracted from lavandin (Lavandula hybrida) flowers using pressurized fluid extraction. A central composite design was used to optimize the effective extraction variables. The chemical composition of extracted samples was analyzed by a gas chromatograph-flame ionization detector column. For achieving 100% extraction yield, the temperature, pressure, extraction time, and the solvent flow rate were adjusted at 90.6°C, 63 bar, 30.4 min, and 0.2 mL/min, respectively. The results showed that pressurized fluid extraction is a practical technique for separation of constituents such as 1,8-cineole (8.1%), linalool (34.1%), linalyl acetate (30.5%), and camphor (7.3%) from lavandin to be applied in the food, fragrance, pharmaceutical, and natural biocides industries.
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Steven B. Hawthorne, Carol B. Grabanski, Esther Martin · Journal of Chromatography A · 2000 · 431 citations
Engineering, Environmental Engineering, Analytical Chemistry +11