Electroanalysis · 2020 · 25 citations · 45 references
PharmacyChemistryAnalytical ChemistryElectrochemistrySensorsElectrochemical CellsElectrochemical DetectionElectrochemical Impedance SpectroscopyElectrochemical SensorsElectrode MaterialsIon-selective ElectrodesBiochar MaterialsDetectionElectrochemical Impedance AnalysisLinear RangePyrolysisRaman SpectraSquare-wave VoltammetryVoltammetry
Abstract Hierarchical porous tubular biochar (PTBC) was prepared by selectively removing lignin simply according to reverse the pyrolysis sequence of cellulose. The properties of the PTBC sample were characterized by XRD, SEM, TEM, Raman spectra, cyclic voltammetry and electrochemical impedance spectroscopy. The electrochemical performances of PTBC modified on the screen‐printing electrode illustrated excellent detection of lead ions (lead (II)) in water with the linear range (0.5–120 μg/L) and the detection limit (0.02 μg/L) by in‐situ bismuth film square wave anode stripping voltammetry.
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