International Journal of Electrochemical Science · 2020 · 10 citations · 29 references
Natural SciencesMaterials EngineeringMaterials ScienceElectrochemistryMetallurgyNanomaterialsElectrode MaterialsMachiningWorking ElectrodesCurrent DensityElectrode FabricationElectrodepositionFine-grained MicrostructureMicrostructureNanocrystalline MaterialsNanostructured Electrode Materials
A nanocrystalline copper electrode material was fabricated using the pulse jet electrodeposition method on a stainless steel rod. The microstructure evolution and grain size were examined using scanning electron microscopy and X-ray diffraction. The nanocrystalline copper had a fine microstructure comprising nanosized grains with a size of 28 nm at a peak current density of 400 A/dm 2 and a pulse duty circle of 1:6. An electrode material mass loss experiment was conducted between the nanocrystalline copper electrode prepared by pulse jet electrodeposition and a conventional electroformed coarse copper electrode. The results show that the relative mass loss factor of the pulse jet electrodeposited copper electrode was obviously lower than that of electroformed coarse copper and reached a minimum value of 0.25% with an applied EDM peak current density of 3 A /dm 2 .
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Ibrahem Maher, Ahmed A. D. Sarhan, M. Hamdi · The International Journal of Advanced Manufacturing Technology · 2014 · 119 citations · Full text