Microsystems & Nanoengineering · 2017 · 26 citations · 43 references
EngineeringMaterials EngineeringMaterials ScienceMaterials CharacterizationNanotechnologySensorsGas SensorsMicroelectromechanical SensorsNanomechanicsOptical SensorsScanning Probe MicroscopySensor MaterialsCantilever Deflection DetectionFilm StressGas SensingInstrument Detection LimitMicrocantilever SensorsStressTest Equipment CalibrationThin Film Mechanics
Hydrogen has attracted attention as an alternative fuel source and as an energy storage medium. However, the flammability of hydrogen at low concentrations makes it a safety concern. Thus, gas concentration measurements are a vital safety issue. Here we present the experimental realization of a palladium thin film cantilever optomechanical hydrogen gas sensor. We measured the instantaneous shape of the cantilever to nanometer-level accuracy using diffraction phase microscopy. Thus, we were able to quantify changes in the curvature of the cantilever as a function of hydrogen concentration and observed that the sensor's minimum detection limit was well below the 250 p.p.m. limit of our test equipment. Using the change in curvature versus the hydrogen curve for calibration, we accurately determined the hydrogen concentrations for a random sequence of exposures. In addition, we calculated the change in film stress as a function of hydrogen concentration and observed a greater sensitivity at lower concentrations.
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Edward M. Eyring · Nuclear Technology · 1978 · 1.3K citations
Diffraction phase microscopy for quantifying cell structure and dynamics
Gabriel Popescu, Takahiro Ikeda, Ramachandra R. Dasari et al. · Optics Letters · 2006 · 818 citations
A hydrogen−sensitive MOS field−effect transistor
Ingemar Lundström, Shriram Shivaraman, C. Svensson et al. · Applied Physics Letters · 1975 · 735 citations