Tuning the instrument resolution using chopper and time of flight at the small-angle neutron scattering diffractometer KWS-2

Aurel Rădulescu, Noemi Szekély, Stephan Polachowski, Marko Leyendecker, Matthias Amann, Johan Buitenhuis, M. Drochner, R. Engels, Romuald Hanslik, Günter Kemmerling,

Journal of Applied Crystallography · 2015 · 28 citations · 14 references

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Abstract

Following demand from the user community regarding the possibility of improving the experimental resolution, the dedicated high-intensity/extended <i>Q</i>-range SANS diffractometer KWS-2 of the Jülich Centre for Neutron Science at the Heinz Maier-Leibnitz Center in Garching was equipped with a double-disc chopper with a variable opening slit window and time-of-flight (TOF) data acquisition option. The chopper used in concert with a dedicated high-intensity velocity selector enables the tuning at will of the wavelength resolution Δλ/λ within a broad range, from 20% (standard) down to 2%, in a convenient and safe manner following pre-planned or spontaneous decisions during the experiment. The new working mode is described in detail, and its efficiency is demonstrated on several standard samples with known properties and on a completely new crystallizable copolymer system, which were investigated using both the conventional (static) and TOF modes.

References

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