Angewandte Chemie International Edition · 2005 · 228 citations · 31 references
Natural SciencesChemical EngineeringChemistryAnalytical ChemistryElectrochemistryReaction EngineeringChemical OxidationHigh-temperature OxidationOxidation AnalysisOxidation-reduction ReactionsRedox ChemistryRedox-active MaterialsAdvanced Oxidation ProcessesHigh-temperature Oxidation ProductsHigh-temperature Oxidation ThermodynamicsLow-temperature OxidationOxidation KineticsOxidation MechanismsOxidation ThermodynamicsTemperature-programmed Oxidation
Residence time controlled reaction: The Swern oxidation of alcohols has been accomplished by using a microscale flow system, consisting of micromixers and microscale tube reactors (see schematic representation; DMSO=dimethylsulfoxide, TFAA=trifluoroacetic anhydride), at higher temperatures (−20 to 20 °C) than those for conventional macroscale batch systems (−50 °C or below).
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