Acta Crystallographica · 1966 · 304 citations · 0 references
Natural SciencesChemistryCrystal StructureStructural BiochemistryStructural BiologyCrystal ChemistryCrystallographyMolecular StructureStructure DeterminationX-ray CrystallographyX-ray DiffractionCrystal Structure DeterminationCrystal Structure RefinementProtein CrystallographyStructure SolutionUnit Cell DeterminationX-ray Crystallographic RefinementX-ray Crystallography Of Amino AcidsX-ray Crystallography-based Structure Determination
The crystal structure of L-alanine, C3H702N, has been determined and refined by analysis of complete three-dimensional diffraction data from copper X-radiation. The crystals are orthorhombic with space group P212~21 ; the unit-cell dimensions are a = 6.032, b = 12.343, c = 5.784 A. Least-squares refinement of the positional parameters of all 13 atoms and of the individual anisotropic temperature factors of the six heavy atoms, using 581 observed reflections of non-zero weight, yielded a final R index of 0.049.