Acquisition Regime for High‐Resolution Heteronuclear 2D NMR Spectra

Abstract

Double take: In the acquisition regime presented here, 1H,13C HSQC spectra are recorded twice with spectral widths of 5.8 and 6.2 ppm in the indirect dimension. The aliased signals are then unfolded to the full spectral width to yield an HSQC spectrum with 5 Hz per point in the 13C dimension without additional time requirements (see example of strychnine). Supporting information for this article is available on the WWW under http://www.wiley-vch.de/contents/jc_2002/2006/z603036_s.pdf or from the author. Please note: The publisher is not responsible for the content or functionality of any supporting information supplied by the authors. Any queries (other than missing content) should be directed to the corresponding author for the article.