Characterization of Thermally Reduced Graphene Oxide by Imaging Ellipsometry

Inhwa Jung, M. Vaupel, Matthew Pelton, Richard D. Piner, Dmitriy A. Dikin, Sasha Stankovich, Jinho An, Rodney S. Ruoff

The Journal of Physical Chemistry C · 2008 · 223 citations · 24 references

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Abstract

The dispersion functions for the refractive index and the extinction coefficient of single- and multiple-layer graphene oxide samples were measured by imaging spectroscopic ellipsometry in the wavelength range of 350−1000 nm and were compared to previously reported results measured by confocal microscopy. The dispersion functions for thin platelets were also compared to those obtained by standard spectroscopic ellipsometry on a deposit consisting of many overlapping graphene oxide layers. Changes were observed in both the thickness of the deposits and the values of the dispersion parameters following heating. A model is proposed to explain these observations, based on the removal of water between the graphene-oxide layers upon thermal treatment.

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