Ultrasound-assisted preparation, characterization and properties of porous Cu<sub>2</sub>O microcubes

Hua Li, Yonghong Ni, Yafei Cai, Li Zhang, Junzhi Zhou, Jianming Hong, Xian‐Wen Wei

Journal of Materials Chemistry · 2008 · 25 citations · 16 references

Concepts

Abstract

Porous Cu2O microcubes have been successfully synthesized via an in situ ultrasound route at an ultrasound power of 90% for 3 h in the presence of polyvinylpyrrolidone (PVP), employing CuCl2·2H2O, C6H12O6·H2O, trisodium citrate and NaOH as starting reactants. The phase and morphology of the product were characterized by means of powder X-ray diffraction (XRD), energy dispersive spectrometry (EDS), transmission electron microscopy (TEM), and field emission scanning electron microscopy (SEM). The investigations showed that the as-prepared porous Cu2O microcubes possessed good electrochemical properties and could photocatalytically degrade organic dye pyronine B under irradiation with 254 nm UV light, and could obviously restrain the propagation of E. coli.

References

16