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On the formation of (triphenylphosphine)(ethylene)pentamethylcyclopentadienylrhodium(I) in the reaction of diiodo(triphenylphosphine)pentamethylcyclopentadienylrhodium(III) with butane-1,4-bis(magnesium bromide). An example of facile CO cleavage of diethyl ether by an organomagnesium compound