Technical Physics · 2002 · 38 citations · 1 references
Natural SciencesMaterials EngineeringMaterials ScienceNanomaterialsNanotechnologyOptical MaterialsInorganic NanoparticlesMetal Oxide NanomaterialsMetal OxidesNanoporous MaterialsOxide SemiconductorsLaser Pulse DurationMetal Oxide Nanoparticle SynthesisNanopowder ProcessingNanostructured OxidesOxide Solid-state Chemistry
The design and characteristics of a setup for producing metal oxide nanopowders with an output of up to 20 g/h are discussed. The grain mean size in the powders is 15 nm, and the radiation power consumption is 30—40 (W h)/g. Y 2 O 3 -stabilized ZrO 2 (YSZ) and Al 2 O 3 + YSZ nanopowders are prepared by target evaporation with a pulse-periodic CO 2 laser, followed by vapor condensation in an air stream. The mean power, peak power, and efficiency of the pulse-periodic CO 2 laser, excited by a combined discharge, are, respectively, 1 kW, 10 kW, and ≈10%. Data for the powder specific surface, grain shape, and grain size distribution, as well as results of X-ray phase and structure analysis, are reported.
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Yu. A. Kotov, R. F. Boehme, G. Schumacher · Materials science forum · 1996 · 18 citations · Full text
Natural Sciences, Materials Engineering, Materials Science +11