A Tutorial on Near Infrared Spectroscopy and Its Calibration

Lidia Esteve Agelet, Charles R. Hurburgh

Critical Reviews in Analytical Chemistry · 2010 · 256 citations · 58 references

Concepts

TL;DR

Near‑infrared spectroscopy has expanded from its 1960s grain‑industry origins to widespread use in materials science, food, environment, medicine, pharmaceutics, agriculture, and archaeology, with continued instrumentation evolution expected. This review serves as a beginner’s guide to NIR. The review covers NIR theory, instrumentation, and calibration stages in a non‑mathematical way, highlighting key operational processes for new users.

Abstract

Near infrared spectroscopy (NIRS) has had rapid usage growth since its first application in the 1960s in the grain industry. Since then, material science, food, environment, medicine, pharmaceutics, agriculture, archeology, and others have reported successful applications of near infrared technologies. Evolution and improvement of instrumentation is expected to continue with increasing users and applications. This review provides a guide for NIR beginners. Theory of NIR measurements, instrumentation, and stages of calibration development are covered in a non-mathematical approach, focusing on critical operating processes to provide new users a starting point for application and study.

References

58