Quantitative Analysis of Gross Adhesive Penetration in Wood Using Fluorescence Microscopy

Abstract

Abstract An optimum amount of adhesive penetration is desirable for economy of production and development of bond strength in wood composites. A general method that allows quantitative measurement of gross adhesive penetration in wood is described. Staining techniques have been developed that can provide sharp contrast between a cured adhesive and the wood substrate using fluorescence microscopy. An image analysis system utilizes this contrast to quantify gross adhesive penetration in wood. An example of this technique is provided, whereby the effect of molecular weight distribution of phenol formaldehyde prepolymers on gross adhesive penetration into yellow poplar (Liriodendron tulipifera) flakes is observed and quantified. Adhesive penetration into wood flakes was shown to be correlated with the molecular weight distribution of the prepolymer, decreasing with higher weight average molecular weight. Gross adhesive penetration into hardwoods is likely to be dominated by flow into vessel elements, as demonstrated by the wood species studied here.