Crystal structure of di[potassium([2.2.2]crypt)]tetrapotassium octadecagermanide(6–)—ethylenediamine solvate (1:6), [K(C18H36N2O6)]2K4(Ge9)2 · 6C2N2H8

Abstract

Abstract C 24 H 60 Ge 9 K 3 N 8 O 6 , triclinic, P 1̅ (No. 2), a = 9.408(2) Å, b = 13.606(3) Å, c = 19.507(4) Å, α = 84.74(3)°, β = 81.35(3)°, γ = 80.18(3)°, V = 2426.8 Å 3 , Z = 2, R gt (F) = 0.064, wR ref (F 2 ) = 0.192, T = 150 K.