Journal of Synchrotron Radiation · 1998 · 13 citations · 5 references
Natural SciencesMaterials EngineeringMaterials ScienceMaterials CharacterizationMechanical Behavior Of MaterialsSurface ScienceStrain AnalysisSurface CharacterizationSurface CrystallographySurface PhysicsX-ray DiffractionX-ray OpticsBragg DiffractionNative Oxide LayersStrain Field MeasurementTotal Internal ReflectionX-ray Diffraction AnalysisX-ray Diffraction Strain Analysis
A new X-ray diffraction technique has been developed in order to measure the strain field near a solid surface under ultrahigh vacuum (UHV) conditions. The X-ray optics use an extremely asymmetric Bragg-case bulk reflection. The glancing angle of the X-rays can be set near the critical angle of total reflection by tuning the X-ray energy. Using this technique, rocking curves for Si surfaces with different surface structures, i.e. a native oxide surface, a slightly oxide surface and an Si(111) 7 x 7 surface, were measured. It was found that the widths of the rocking curves depend on the surface structures. This technique is efficient in distinguishing the strain field corresponding to each surface structure.
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