Publication | Closed Access
Automated Parallel Synthesis of MADIX (Co)Polymers
45
Citations
12
References
2003
Year
EngineeringPolymer LibrariesParallel SynthesisChemistryParallel PolymerizationsPolymersMacromolecular EngineeringAutomated Madix PolymerizationsPolymer ProcessingPrecision MacromoleculePolymer ChemistryMaterials ScienceSynthetic MacromoleculeDiversity-oriented SynthesisSynthesis MethodBiomolecular EngineeringNatural SciencesPolymer SciencePolymer CharacterizationPolymerization KineticsPolymer ReactionPolymer Synthesis
Abstract An automated parallel synthetic approach has been developed for synthesizing polymer libraries by the Macromolecular Design via the Interchange of Xanthates (MADIX) process. The experimental set‐up, parallel polymerizations, characterization, and reproducibility tests are detailed. Examples of acrylic diblock copolymers synthesized in this way are given. Automated MADIX polymerizations of BA in the presence of a X 1 ‐capped PEA. magnified image Automated MADIX polymerizations of BA in the presence of a X 1 ‐capped PEA.
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