Carbon-13 nuclear magnetic resonance spectra of phytoecdysones.

Hiroshi Hikino, Toru Okuyama, Chohachi Konno, Tsunematsu Takemoto

Chemical and Pharmaceutical Bulletin · 1975 · 32 citations · 0 references

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Abstract

The natural-abundance 13C nuclear magnetic resonance spectra of certain phytoecdysones and their selected derivatives have been measured at 25 MHz. With the aid of complete noise, off-resonance, and single-frequency proton decoupling techniques, and the shifts which occur on formation of specific derivatives, it has been possible to make assignments of the resonances for the phytoecdysones.