Crystal structure of diaqua-bis(μ₂-6-phenylpyridine-2-carboxylate-κ³N,O:O)-bis(6-phenylpyridine-2-carboxylato-κ²N,O)lead(II) – <i>N,N</i>-dimethylformamide – water (1/2/4), C₅₄H₅₈N₆O₁₆Pb₂

Abstract

Abstract C 54 H 58 N 6 O 16 Pb 2 , triclinic, <m:math xmlns:m="http://www.w3.org/1998/Math/MathML" overflow="scroll"> <m:mrow> <m:mi>P</m:mi> <m:mover accent="true"> <m:mn>1</m:mn> <m:mo stretchy="true">‾</m:mo> </m:mover> </m:mrow> </m:math> $P&amp;#x203e;{1}$ (no. 2), a = 9.4690(6) Å, b = 12.9374(6) Å, c = 13.2303(7) Å, V = 1341.90(15) Å 3 , α = 63.395(5)°, β = 74.291(5)°, γ = 69.113(5)°, Z = 1, R gt ( F ) = 0.0284, wR ref ( F 2 ) = 0.0484, T = 150 K.