Micromachines · 2021 · 58 citations · 27 references
Natural SciencesMaterials EngineeringMaterials ScienceAdditive ManufacturingMagnetic MaterialsMetallurgyAlloysFerromagnetic MaterialsFerromagnetismMagnetic Properties Of SolidsPermanent MagnetsPowder Bed FusionAdditive Manufacturing PowdersAdditive Manufacturing SolidificationLaser Powder Bed FusionMagnetic CoercivityMagnetic PropertiesNanocrystalline Magnetic MaterialsNanocrystalline MagnetsSelective Laser Melting
Lab scale additive manufacturing of Fe-Nd-B based powders was performed to realize bulk nanocrystalline Fe-Nd-B based permanent magnets. For fabrication a special inert gas process chamber for laser powder bed fusion was used. Inspired by the nanocrystalline ribbon structures, well-known from melt-spinning, the concept was successfully transferred to the additive manufactured parts. For example, for Nd16.5-Pr1.5-Zr2.6-Ti2.5-Co2.2-Fe65.9-B8.8 (excess rare earth (RE) = Nd, Pr; the amount of additives was chosen following Magnequench (MQ) powder composition) a maximum coercivity of µ0Hc = 1.16 T, remanence Jr = 0.58 T and maximum energy density of (BH)max = 62.3 kJ/m3 have been achieved. The most important prerequisite to develop nanocrystalline printed parts with good magnetic properties is to enable rapid solidification during selective laser melting. This is made possible by a shallow melt pool during laser melting. Melt pool depths as low as 20 to 40 µm have been achieved. The printed bulk nanocrystalline Fe-Nd-B based permanent magnets have the potential to realize magnets known so far as polymer bonded magnets without polymer.
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