Rare Metals · 2020 · 22 citations · 25 references
Natural SciencesMaterials EngineeringMaterials ScienceMetallurgyPhase TransformationsSolid State PhysicsAlloysGrain Structure FormationKinetics Of Phase TransformationsMetalsMicrostructure EvolutionPhase AnalysisAlloy Phase DiagramsElectron Beam MeltingMelting Of AlloysPhase Diagram DesignTitanium AlloysTitanium Metallurgy
Abstract It is important to understand the correlation between grain morphology and intervariant boundaries of the α phase after heat treatment below β transus of the electron beam melted (EBMed) Ti–6Al–4V alloy. Scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) analysis have shown about 99% α phase and 1% β phase in the heat‐treated samples when the temperature rises to 950 °C. Four distinct types of α grain morphology have been found: allotromorphous α, relatively coarse α plate, large precipitation α and granular α. A single peak of the intervariant boundary with the misorientation of 60°/ associated with Burgers orientation relationship (OR) was found in the allotromorphous α colony. Multiple intervariant boundaries mixed with a fraction of general high‐angle grain boundary (GHABs, not Burgers OR) were present in the relatively coarse α plate colony. Almost only low‐angle grain boundaries (LABs) with the misorientation of < 5° were found in the large precipitation α grains. β phase tends to distribute around the boundaries of relatively coarse α plates. It suggests that different formation mechanisms are involved in the distinct types of α grain morphology.
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