Scientific Reports · 2020 · 320 citations · 35 references
Natural SciencesMaterials EngineeringMaterials ScienceBiomedical ImagingDiagnostic ImagingOpticsElectron DiffractionX-ray DiffractionX-ray OpticsBragg DiffractionCoherent ImagingDiffraction ImagingScan Time ReductionStrain FieldsX-ray Imaging Physics
Continuous scanning reduces sample instability under the beam and will be increasingly important at diffraction‑limited storage ring light sources. The study explores using continuous scanning during data acquisition for Bragg coherent diffraction imaging, where the sample moves continuously. The authors implement continuous scanning during Bragg coherent diffraction imaging by moving the sample continuously during data acquisition. Continuous scanning Bragg coherent diffraction imaging on a Pt nanoparticle at 400 °C in an Ar flow reduced scan time by 30 % and produced Bragg electron density, phase, displacement, and strain fields that agree well with conventional step‑by‑step scanning.
Abstract We explore the use of continuous scanning during data acquisition for Bragg coherent diffraction imaging, i.e., where the sample is in continuous motion. The fidelity of continuous scanning Bragg coherent diffraction imaging is demonstrated on a single Pt nanoparticle in a flow reactor at $$400\,^\circ \hbox {C}$$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:mrow> <mml:mn>400</mml:mn> <mml:msup> <mml:mspace/> <mml:mo>∘</mml:mo> </mml:msup> <mml:mtext>C</mml:mtext> </mml:mrow> </mml:math> in an Ar-based gas flowed at 50 ml/min. We show a reduction of 30% in total scan time compared to conventional step-by-step scanning. The reconstructed Bragg electron density, phase, displacement and strain fields are in excellent agreement with the results obtained from conventional step-by-step scanning. Continuous scanning will allow to minimise sample instability under the beam and will become increasingly important at diffraction-limited storage ring light sources.
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Reconstruction of an object from the modulus of its Fourier transform
James R. Fienup · Optics Letters · 1978 · 1.8K citations
X-ray image reconstruction from a diffraction pattern alone
Stefano Marchesini, Haifeng He, Henry N. Chapman et al. · Physical review. B, Condensed matter · 2003 · 874 citations · Full text