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Palladium-Mediated Reductive Heck Cyclization for the Formation of Dibenzoazepinone Framework
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2009
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Cross-coupling ReactionEngineeringHeterocyclicReductive Heck CyclizationPalladium-mediated Sonogashira Cross-couplingDibenzoazepinone FrameworkOrganic ChemistryOrganometallic CatalysisChemistryBiomolecular Engineering
The dibenzoazepinone framework has been synthesized through a palladium-mediated Sonogashira cross-coupling followed by a reductive Heck cyclization. The reactions are simple, straightforward, and have been carried out under ligand-free conditions.