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Improved Synthesis of Benzotriazoles and 1-Acylbenzotriazoles by Ultrasound Irradiation
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2007
Year
Ultrasoundassisted PreparationEngineeringHeterocyclicPower UltrasoundSonoelectrochemistrySonochemistryOrganic ChemistryChemistryUltrasoundUltrasound IrradiationSodium NitriteHeterocycle ChemistryDerivative (Chemistry)Acetic Acid
Some 1H-benzotriazoles have been synthesised in good yields in short times by reaction of ophenylenediamine with sodium nitrite in acetic acid under ultrasound irradiation. Also, the ultrasoundassisted preparation of 1-acylbenzotriazoles is described. Keywords: Benzotriazoles, acylbenzotriazoles, ultrasound irradiation, sonochemistry, heterocycles