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Reduction of Aromatic Ketones into Methylenes Using Triethylsilane and Titanium Tetrachloride. Synthesis of 2-Aminobutanoic Acids
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1995
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Organic Material ChemistryChemical EngineeringEngineeringMethylenes Using TriethylsilanePhotochemistryAromatic KetonesC F 3Organic Chemistry2-Aminobutanoic AcidsChemistryOptical PuritySynthetic ChemistryEnantioselective SynthesisHplc Analysis.7
5. Reduction of ethyl 4-(4chlomphenyl)-2-(methoxycarbony1amino)4o~ob~tanoate with Et3SiH in boiling C F 3 W gave ethyl 4-(4-chlomphenyl)-2-(methoxycarbony1amino)butanoate in only 15% yield 6. Optical purity of the product was determined by hplc analysis.7.