Supramolecular Fe<sub>3</sub>O<sub>4</sub>@PEG/−diaza crown ether@Ni: a novel magnetically reusable nano catalyst for the clean synthesis of 2‐aryl‐2,3‐dihydroquinazolin‐4(1<i>H</i>)‐ones

Michael Aalinejad, Nader Noroozi Pesyan, Nosrat Heidari, Hana Batmani, Aria Danandeh Asl

Applied Organometallic Chemistry · 2019 · 16 citations · 40 references

Concepts

Abstract

Ni@diaza crown ether complex supported on magnetic nanoparticle was provided by grafting technique. The catalytic activity of Fe 3 O 4 @diaza crown ether@Ni was explored through one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1 H )‐ones and it was used as an efficient and recoverably constant nanocatalyst. FT‐IR, SEM, TEM, XRD, BET, ICP, EDS, and TGA techniques were employed to specify the nanocatalyst. This heterogeneous catalyst demonstrated acceptable recyclability and could be used again several times with no considerable loss of its catalytic activity.

References

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