Synthesis, characterization and application of nano‐CoAl₂O₄ as an efficient catalyst in the preparation of hexahydroquinolines

Abstract

In this work, nano‐CoAl 2 O 4 was prepared and characterized by FT‐IR, energy dispersive X‐ray analysis (EDX), X‐ray diffraction patterns (XRD), scanning electron microscopy (SEM), vibrating sample magnetometer (VSM) and transmission electron microscopy (TEM). Nano‐CoAl 2 O 4 was applied for the synthesis of hexahydroquinoline derivatives by the condensation reaction between ethyl acetoacetate, dimedone and various aldehydes. These reactions were carried out at 80 °C under solvent‐free conditions.