Publication | Closed Access
PhSO<sub>2</sub>SCF<sub>2</sub>H: A Shelf‐Stable, Easily Scalable Reagent for Radical Difluoromethylthiolation
130
Citations
46
References
2016
Year
A new shelf-stable and easily scalable difluoromethylthiolating reagent S-(difluoromethyl) benzenesulfonothioate (PhSO<sub>2</sub> SCF<sub>2</sub> H) was developed. PhSO<sub>2</sub> SCF<sub>2</sub> H is a powerful reagent for radical difluoromethylthiolation of aryl and alkyl boronic acids, decarboxylative difluoromethylthiolation of aliphatic acids, and a phenylsulfonyl-difluoromethylthio difunctionalization of alkenes under mild reaction conditions.
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