2002 · 30 citations · 10 references
EngineeringMaterials EngineeringMaterials ScienceElectronic MaterialsMicroelectromechanical SystemsThin FilmsFabrication MaterialsMems MaterialsMems ResonatorsRf MemsThin Film AnnealingThin Film Mechanical PropertiesElastic ModulusQuality Factor MeasurementRapid Thermal AnnealingResonance FrequenciesRf Mems ResonatorsSiliconStrain GradientThermal Annealing
This paper presents new material data for single-and multilayer CMOS compatible poly-SiGe films, including mechanical quality factor (Q), Young's modulus, and strain gradient. Using audio frequency folded-flexure comb-drive resonators, the mechanical quality factor of poly-SiGe was determined at 2Torr pressure. As-deposited poly-SiGe has Q = 20,000 -31,000. CMOS compatible rapid thermal annealing (RTA) at 525C for 60 seconds results in a quality factor between 40,000 and 44,000. We have measured the highest Q factor yet reported for poly-SiGe (Q 61,100), as a result of RTA at 600C for one minute. The measured resonant frequencies of the resonators were used to back-calculate the Young's modulus of poly-SiGe: E = 155 5GPa. The calculated elastic modulus is significantly higher than the metallurgical Young's modulus of 146GPa. The as-deposited strain gradient of the tri-layer poly-SiGe film was found to be 1.7510 -4 m -1 (curl-up). RTA at 600C for one minute drops the tri-layer strain gradient to 2.6710 -5 m -1 (curl-up). The graded Ge content multi-layer film was observed to induce a larger normalized strain gradient.
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