Publication | Closed Access
Silver(I)-Catalyzed Deprotection of <i>p</i>-Methoxybenzyl Ethers: A Mild and Chemoselective Method
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Citations
57
References
2012
Year
Chemoselective MethodChemical EngineeringVarious AlcoholsEngineeringCatalytic AmountOrganic ChemistryOrganometallic CatalysisCatalysisSynthetic ChemistryChemistryP-methoxybenzyl Protecting GroupCatalytic Synthesis
The p-methoxybenzyl protecting group (PMB) on various alcohols and an acid was efficiently and selectively cleaved by the action of a catalytic amount of silver(I) hexafluoroantimonate combined with 0.5 equiv of 1,3,5-trimethoxybenzene in dichloromethane at 40 °C.
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