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Preparation of nanocrystalline thin films of ZnO by sol-gel dip coating
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2011
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EngineeringSol Gel MethodNanocrystalline Thin FilmsHexagonal Crystal StructureThin Film Process TechnologySol-gel SynthesisNanoengineeringFilm SurfaceNanostructure SynthesisThin Film ProcessingMaterials ScienceNanotechnologyOxide ElectronicsOxide SemiconductorsSol-gel Dip CoatingNanocrystalline MaterialNanomaterialsApplied PhysicsThin Films
doping (0, 1, 5, 10 and 15 wt%) are prepared for the first time by the sol gel method. The film surface is with a ganglia-like structure as observed by Scanning Electron Microscopy (SEM). The films comprise of ZnO nanocrystallites with hexagonal crystal structure, as revealed by means of X-ray diffraction (XRD). (ii) Films on aluminium foil substrates. The ZnO films are annealed at different temperatures (100 °C, 300 °C and 500 °C) and characterized by means of SEM and XRD. The film surface is with the characteristic ganglia-like patterns. The crystalline structure is hexagonal with the crystallite sizes increasing with the annealing temperature.