Publication | Closed Access
A Convenient Preparation of Trimethylborane and Triethylborane
78
Citations
3
References
1973
Year
Materials ScienceInorganic ChemistryDerivative (Chemistry)EngineeringConvenient PreparationLaboratory ScaleOrganic ChemistryHigh Yield PreparationPilot Plant ScaleCatalysisChemistryChemical DerivativeInorganic Synthesis
Abstract A convenient, high yield preparation of Me3B on a laboratory scale from (n-BuO)3B and Me3Al2Cl3 is described. The preparation of Et3B from Al3Et and Et2O[sbnd]BF3 on a laboratory scale and from AlEt3 and KBF4 on a pilot plant scale are also given.
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