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Gram-Scale Preparation of VAPOL Hydrogenphosphate: A Structurally Distinct Chiral Brønsted Acid
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2010
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High YieldsAsymmetric CatalysisEngineeringNatural SciencesDiversity-oriented SynthesisOrganic ChemistryGram-scale PreparationDetailed Gram-scale SynthesisStereoselective SynthesisChemistrySynthesis MethodVapol HydrogenphosphateSynthetic ChemistryEnantioselective SynthesisBiomolecular Engineering
A detailed gram-scale synthesis of VAPOL hydrogenphosphate, a structurally distinct chiral Brønsted acid, is presented. The reaction utilizes commercially available starting materials, proceeds with high yields and has been reproduced numerous times at scale.