DergiPark (Istanbul University) · 2003 · 31 citations · 0 references
Natural SciencesChemistryEnvironmental SciencesAnalytical ChemistryElemental AnalysisInorganic ChemistryEnvironmental Analytical ChemistryEnvironmental Elemental AnalysisExtraction TechniquesHeavy Metal AnalysisHeavy Metal ContaminationInstrumental AnalysisAnalytical Detection Of Heavy MetalsChelation-based Mineral AnalysisEnrichmentFlame Atomic Absorption SpectrometryFlame Atomic Absorption SpectroscopyMetal ExtractionPre-concentrationSpeciation In Water Samples
A solid-phase extraction method was developed for the pre-concentration of manganese, copper, cadmium and lead in water samples prior to their determination by flame atomic absorption spectrometry using phenylpiperazine dithiocarbamate as a new reagent. The optimum pre-concentration conditions have been investigated such as pH, volume of sample solution and the effects of some matrix elements. The obtained recovery was nearly 90 to 100, while the enrichment factor was 400 for metal spiked solutions.