IEEE Transactions on Applied Superconductivity · 2003 · 58 citations · 11 references
Natural SciencesMaterials EngineeringMaterials ScienceMetallic MaterialsSurface ScienceThin FilmsMetal MaterialsMetalsSuperconducting Thin FilmsThin Film Surface MorphologyThin-film DepositionX-ray DiffractionDeposition TechniquesFilm Growth MechanismsReflection High-energy Electron DiffractionSubstrate Surface PreparationSuperconducting CeramicsThin Film Growth MonitoringThin-film Growth MechanismsX-ray Diffraction Analysis
We present our results to improve ion beam assisted deposition (IBAD) of magnesia (MgO) templates for subsequent YBa/sub 2/Cu/sub 3/O/sub 7-/spl delta// (YBCO) deposition. The substrate surface roughness has a significant effect on the initial nucleation texture of IBAD MgO films. We have found that reduction in our substrate surface roughness to /spl sim/ 3.5 nm has resulted in better in-plane texture for IBAD MgO films than those deposited on rougher metal substrates. We have further improved the IBAD MgO deposition parameters by using an in situ reflected high-energy electron diffraction (RHEED) analysis tool that allows for monitoring of IBAD MgO growth. We have found a direct correlation between the RHEED generated intensity versus time curve and in-plane texture. Utilizing X-ray diffraction analysis, we have been able to determine the optimum deposition parameters to routinely grow films in batch mode that have a phi scan /spl Delta//spl phi/ from 6 - 7/spl deg/. Coupling the improvements in substrate preparation with optimization of IBAD MgO deposition has allowed for both batch and continuous deposition (termed c-IBAD MgO) on metallic substrates that result in superior superconducting properties. We have demonstrated that deposited meter lengths have had phi scan FWHM values from 8 - 9/spl deg/ with /spl plusmn/ 10% uniformity. Additionally, we have been able to widen the processing zone in our system and coat two, one-meter lengths simultaneously while preserving good texture quality (/spl Delta//spl phi//sub ave/ /spl sim/ 8/spl deg/) and uniformity (60 - 80% of tape length within /spl plusmn/ 5% of /spl Delta//spl phi//sub ave/) for both tapes.
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C. P. Wang, M. R. Beasley, T. H. Geballe et al. · Applied Physics Letters · 1997 · 314 citations
Natural Sciences, Materials Engineering, Materials Science +17
R. P. Reade, Paul Berdahl, R. E. Russo et al. · Applied Physics Letters · 1992 · 265 citations
Natural Sciences, Materials Engineering, Materials Science +11
Coated conductor development: an assessment
D. K. Finnemore, K. E. Gray, M. P. Maley et al. · Physica C Superconductivity · 1999 · 74 citations
Natural Sciences, Materials Engineering, Materials Science +5