IOSR Journal of Applied Chemistry · 2014 · 20 citations · 3 references
Natural SciencesEarth SciencesSoil SciencesElemental AnalysisMineralogySoil ChemistryClay MineralogyClay MineralsIron OxidesMineral ChemistryMineral GeochemistryMineral IdentificationClay Mineral AnalysisClaysEnergy Dispersive X-ray SpectroscopyEnergy-dispersive X-ray SpectroscopyMineral Phase IdentificationQualitative Composition AnalysisX-ray Diffraction AnalysisX-ray Fluorescence Spectroscopy
The characterization of some Nigerian clay deposits has been carried out by employing fourdifferent characterization techniques.The relative proportions of the constituent compounds, the morphology and the phase identification of the different clays were determined by using X-Ray Fluorescence (XRF), Scanning Electron Microscopy/Energy Dispersive Spectroscopy (SEM/EDS), X-Ray Diffraction (XRD)and Transmission Electron Microscopy (TEM)analyses. The clays obtained from the various deposits were prepared for the analyses, using the standard procedure and the results obtained were compared to confirm the consistency and reliability of the different methods employed. The results obtained revealed the various desirable (S i O 2 and Al 2 O 3 ) and deleterious (Fe 2 O 3, K 2 O and MgO) compounds contained in the clay samples, in the various proportions. The appropriate purification technique necessary for preparing the clays for refractory applications were therefore identified.
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