Journal of Microscopy · 1975 · 1.8K citations · 3 references
Natural SciencesMaterials EngineeringMaterials ScienceAnalytical ChemistryRadiation DetectionRadiation MeasurementElectron MicroscopyX-ray DetectionX-ray DetectorsX-ray OpticsX-ray ProductionX-ray SpectroscopyCalibration Curve AnalysisCalibration Curve FittingEnergy Dispersive X-ray SpectroscopyEnergy-dispersive DetectionEnergy-dispersive X-ray SpectroscopyExperimental CharacterizationX-ray Diagnostics
SUMMARY Results are reported concerning the use of an energy dispersive X‐ray detector to carry out the analysis of thin foils in the electron microscope. The combination of a thin specimen and the extreme stability of the energy dispersive X‐ray detector enables the experimental determination of a calibration curve of X‐ray production—detection efficiency vs characteristic X‐ray energy. Quantitative analysis can be carried out using the calibration curve without reference to standards at the time of analysis.
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