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Sanguinarine pseudobase: re-examination of NMR assignments using gradient-enhanced spectroscopy

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1998

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Abstract

The formation of sanguinarine pseudobase (6-hydroxydihydrosanguinarine) was studied by 1D and 2D NMR spectroscopy. The unequivocal evidence of a hemiaminal OH group and unambiguous 1H, 13C and 15N NMR assignments of this compound are discussed. © 1998 John Wiley & Sons, Ltd.