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The direct determination of dose‐to‐water using a water calorimeter
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1987
Year
EngineeringDifferential Scanning CalorimetryMeasurementWater CalorimeterExperimental ThermodynamicsRefrigerationCalibrationAnalytical ChemistryThermodynamicsPhysicsWater QualityCalorimetric MethodHeat TransferMultiphase FlowDosimetryWater AnalysisSurrounding WaterEnvironmental EngineeringTemperature MeasurementApplied PhysicsRadiation DoseMedicineThermal EngineeringNested CylindersThermal InsulationDrug Analysis
A flexible, temperature-regulated, water calorimeter has been constructed which consists of three nested cylinders. The innermost "core" is a 10 X 10 cm right cylinder made of glass, the contents of which are isolated from the environment. It has two Teflon-washered glass valves for filling, and two thermistors are supported at the center by glass capillary tubes. Surrounding the core is a "jacket" that provides approximately 2 cm of air insulation between the core and the "shield." The shield surrounds the jacket with a 2.5-cm layer of temperature-regulated water flowing at 51/min. The core is filled with highly purified water the gas content of which is established prior to filling. Convection currents, which may be induced by dose gradients or thermistor power dissipation, are eliminated by operating the calorimeter at 4 degrees C. Depending upon the power level of the thermistors, 15-200 microW, and the insulation provided by the glass capillary tubing, the temperature of the thermistors is higher than that of the surrounding water. To minimize potential errors caused by differences between calibration curves obtained at finite power levels, the zero-power-level calibration curve obtained by extrapolation is employed. Also the calorimeter response is corrected for the change in power level, and therefore thermistor temperature, that follows the resistance change caused by irradiation. The response of the calorimeter to 4-MV x rays has been compared to that of an ionization chamber irradiated in an identical geometry.(ABSTRACT TRUNCATED AT 250 WORDS)