Synthesis and characterization of nanocrystalline graphite from coconut shell with heating process

Frischa M. Wachid, Adhi Y. Perkasa, Fandi Angga Prasetya, Nurul Rosyidah, Darminto Darminto

AIP conference proceedings · 2014 · 42 citations · 3 references

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Abstract

Graphite were synthesized and characterized by heating process of coconut shell with varying temperature (400, 800 and 1000C) and holding time (3 and 5 hours).After heating process, the samples were characterized by X-ray diffraction (XRD) and analyzed by X'pert HighScore Plus Software, Scanning Electron Microcope-Energy Dispersive X-Ray (SEM-EDX) and Transmission Electron Microscope-Energy Dispersive X-Ray (TEM-EDX). Graphite and londsdaelite phase were analyzed by XRD. According to EDX analysis, the sample was heated in 1000C got the highest content of carbon. The amorphous carbon and nanocrystalline graphite were observed by SEM-EDX and TEM-EDX.

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