Science · 1963 · 153 citations · 4 references
Life SciencesBiochemistryChemistryCarbohydrate BiochemistryCarbohydrate ChemistryStructural BiochemistryCrystal ChemistryCrystallographyMacromolecular Structure DeterminationStructural ElucidationStructure DeterminationX-ray CrystallographyCarbohydrate CrystallographyCarbohydrate Structural CharacterizationConformational Analysis Of FuranosesFuranose ConformationHydrogen Bonds In CarbohydratesMolecular Structure DeterminationOligosaccharide CharacterizationSugar Conformation
This analysis provides the first precise molecular parameters for sucrose. All hydrogen atoms are included. Carbon-carbon distances are 1.51 1.53 A; carbon-oxygen 1.40 to 1.44 A; carbon-hydrogen 1.08 to 1.11 A; oxygen-hydrogen 0.94 to 0.99 A. The furanose ring conformation differs from that in sucrose sodium bromide dihydrate. Hydrogen bonds (two of them intramolecular) utilize every hydroxyl group except one.
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OR FLS--A FORTRAN CRYSTALLOGRAPHIC LEAST-SQUARES PROGRAM
W. R. Busing, K. O. Martin, H. A. Levy · 1962 · 276 citations · Full text
The crystal structure of sucrose
C. A. Beevers, T. R. R. McDonald, J. H. Robertson et al. · Acta Crystallographica · 1952 · 85 citations