Nanotechnology · 2011 · 73 citations · 36 references
Natural SciencesMaterials EngineeringMaterials ScienceMaterials CharacterizationNanomaterialsNanotechnologyMetalsNanomechanical PropertiesNanomechanicsNanoscale MaterialsNanowiresTransmission Electron MicroscopyDamage MechanismsMechanical Properties Of NanowiresMetal NanowiresMicromechanical TestingStrain In NanostructuresStress MeasurementTensile StrainTensile Testing
In this paper, we have demonstrated the usage of a novel micro-mechanical device (MMD) to perform quantitative in situ tensile tests on individual metallic nanowires inside a transmission electron microscope (TEM). Our preliminary experiment on a 360 nm diameter nickel nanowire showed that the sample fractured at an engineering stress of ∼ 1.2 GPa and an engineering strain of ∼ 4%, which is consistent with earlier experiments performed inside a scanning electron microscope (SEM). With in situ high resolution TEM imaging and diffraction capabilities, this novel experimental set-up could provide unique opportunities to reveal the underlying deformation and damage mechanisms for metals at the nanoscale.
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