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Electronic Properties and Orientation Studies of Poly‐3‐Alkylselenophene Electrochemically Deposited on Pt As Observed by NEXAFS

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1990

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Abstract

The electronic properties and orientation of films of poly‐3‐alkylselenophenes electrochemically deposited onto Pt have been studied by NEXAFS. The C—K edge characteristics reveal that several major effects occur when n is increased from 0 to 9: (i) In the undoped semiconducting form, a continuous decrease in the polymeric 1s → π* intensity is observed due to an overlap between the π* antibonding band from the polymer and the band which develop when the alkyl chain length increases. (ii) The doping to the conducting state proceeds via a narrowing of the bandgap causing the appearance of metallic‐like behavior. However, the changes in the unoccupied antibonding π* band become less pronounced for a long alkyl chain length. (iii) The orientation of the selenophene ring structure switches from a "lying‐down" to an "on‐edge" configuration with the long alkyl chain being oriented perpendicular to the Pt surfaces.